Journal
TETRAHEDRON
Volume 66, Issue 47, Pages 9304-9309Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2010.09.018
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Funding
- DST
- ICMR India
- CSIR
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Starting from palmityl alcohol divergent stereoselective syntheses of spisulosine and its diastereo- and regio-isomers have been achieved In the Sharpless asymmetric dihydroxylation-based approach the key step is the synthesis of monoprotected diol whereas Miyashita s boron-directed C-2 regioselective azidolysis of enantiomerically pure epoxy alcohol is the vital step in the Sharpless asymmetric epoxidation-based route The latter approach Involves the first protecting-group-free synthesis of spisulosine (C) 2010 Published by Elsevier Ltd
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