Journal
TETRAHEDRON
Volume 65, Issue 29-30, Pages 5716-5719Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2009.05.022
Keywords
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Funding
- NSFC [20621091, 20672048, 20732002]
- '111' program of Chinese Education Ministry.
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An efficient total synthesis of (+/-)-13-epineostenine (2) has been achieved in 15 steps and 17% overall yield. This approach involved the key alkylation/Michael additions of the central 1,4-cyclohexanedione monoethylene acetal and all of the stereocenters on central cyclohexane moiety were generated in highly stereoselectivity. (C) 2009 Elsevier Ltd. All rights reserved.
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