Journal
TETRAHEDRON
Volume 65, Issue 1, Pages 101-108Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2008.10.101
Keywords
Benzopyranobenzopyrans; Naphthopyranobenzopyrans; Aldol-type reaction; Hetero Diels-Alder reaction; Resorcinols; Naphthols
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Funding
- Ministry of Knowledge Economy (MKE) [RT104-01-04]
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The efficient one-pot synthetic approaches for benzopyranobenzopyrans and naphthopyranobenzopyrans are described. The key strategies involve ethylenediamine diacetate-catalyzed cyclization by domino aldol-type reaction/hetero Diels-Alder reaction of resorcinols and naphthols to benzaldehydes with O-allyl ether groups. These reactions provide a rapid route for the synthesis of novel types of poly-heterocycles with stereochemically defined quaternary carbon centers. (C) 2008 Elsevier Ltd. All rights reserved.
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