Journal
TETRAHEDRON
Volume 65, Issue 18, Pages 3773-3779Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2009.02.053
Keywords
Ketalization; Catechol; Benzo[1,3]dioxole; Functional group transformations
Categories
Funding
- German Research Foundation [SFB 624]
- Egyptian Government
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Highly functionalized catechol ketals exhibiting either a tert-butyl moiety or a spiro center in position 2 are synthesized by ketalization and functionalized in a sequence of subsequent transformations. By a specific ketalization protocol catechol ketals of enolizable beta-keto esters can be prepared. With the succeeding steps these compounds incorporate moieties, which are not compatible and accessible by direct ketalization of catechol. (C) 2009 Elsevier Ltd. All rights reserved.
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