Journal
TETRAHEDRON
Volume 64, Issue 25, Pages 5915-5919Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2008.04.039
Keywords
electrolysis; electrocatalysis; carbonyl compounds; nitromethane; Henry reaction; beta-nitroalcohols
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The electrolysis of carbonyl compounds and nitromethane in methanol or in the mixture of methanol and DMF in an undivided cell results in the formation of corresponding beta-nitroalcohols in 60-75% yields. Thus, the simple electrocatalytic system can produce under mild conditions an electrochemically induced Henry reaction. (C) 2008 Elsevier Ltd. All rights reserved.
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