Journal
TETRAHEDRON
Volume 64, Issue 41, Pages 9669-9674Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2008.07.059
Keywords
benzo[b][1,4]thiazin-3(4H)-one; microwave; smiles rearrangement; 2-chlorobenzenethiol; one-pot
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Funding
- SMBA-Korea [2007-S1016568]
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The synthesis of benzo[b][1,4]thiazin-3(4H)-one derivatives in a simple and efficient method from the one-pot reaction of substituted 2-chlorobenzenthiols, chloroacetyl chloride, and primary amines via Smiles rearrangement under microwave irradiation gave high yields (65-92%) of the products with short reaction time (15-20 min). (C) 2008 Published by Elsevier Ltd.
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