Journal
SYNTHETIC COMMUNICATIONS
Volume 43, Issue 21, Pages 2913-2925Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2012.749991
Keywords
Aromatic and heteroaromatic amines; hexamethylene bis(N-methylimidazolium) bis(dichloroiodate); iodination; ionic liquid; terminal alkynes
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Funding
- Research Council of the University of Mazandaran
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Hexamethylene bis(N-methylimidazolium) bis(dichloroiodate) (HMBMIBDCI), an ionic liquid iodinating reagent, have been prepared and characterized. Its ability to perform iodination reactions with a variety of substrates has been explored. In general, iodination reactions of aromatic and heteroaromatic amines proceed with good yields in the absence of solvent. Reactions of terminal alkynes in the presence of 1,8-diazabicyclo [5.4.O] undec-7-ene and tetrahydrofuran have been investigated as well. [Supplementary materials are available for this article. Go to the publisher's online edition of Synthetic Communications (R) for the following free supplemental resource: Full experimental and spectral details.]
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