Journal
SYNTHETIC COMMUNICATIONS
Volume 43, Issue 13, Pages 1772-1777Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2012.667491
Keywords
Diamondoid acetic acids; diamondoids; vinyl derivatives
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Funding
- Ukrainian Basic Research Foundation
- Ministry of Science and Education of Ukraine
- Department of Energy, Office of Basic Energy Sciences, Division of Materials, Science, and Engineering [DE-AC-76SF00515]
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We describe a convenient four-step preparation of 1- vinyl adamantane, 1- vinyl diamantane, and 4,9-divinyl diamantane from the respective diamondoid acetic acids in 50-80% isolated yields involving esterification, reduction, and hydrobromination/dehydrobromination. Supplemental materials are available for this article. Go to the publisher's online edition of Synthetic Communications (R) to view the free supplemental file.
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