Journal
SYNTHETIC COMMUNICATIONS
Volume 42, Issue 11, Pages 1661-1668Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2010.542861
Keywords
Cyanostilbene; cyclotriphosphazene; Knoevenagel condensation; liquid crystal; star-shaped molecule
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Funding
- Natural Science Foundation of China [50703013]
- Independent Innovative Position of Hubei Province
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The synthesis and mesomorphic properties of a class of cyclotriphosphazenes containing cyanostilbene groups with different terminal substituents (-H, -CH3, -OCH3, -CN) are described. All the resulting compounds are characterized by H-1, C-13, and P-31 NMR, matrix-assisted laser desorption/ionization time of flight, and elemental analysis. The thermal behaviors of cyclotriphosphazene derivatives are studied by the means of differential scanning calorimetry and polarizing optical microscopy. Nematic phases are observed in cyclotriphosphazenes with terminal substituents (-CH3, -OCH3, CN).
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