Journal
SYNTHETIC COMMUNICATIONS
Volume 41, Issue 15, Pages 2226-2233Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2010.501474
Keywords
Biginelli-type reaction; BrOnsted acidic ionic liquid; one-pot; pyrimidinone; solvent-free
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Funding
- Isfahan University of Technology (IUT), the government of Iran
- National Institutes of Health [GM 033138, MH 065503, NS 033650]
- Center of Excellency in Sensor and Green Chemistry Research (IUT)
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[image omitted] A mild and efficient method has been developed for the preparation of pyrimidinone derivatives from the reaction of aromatic aldehydes with cyclopentanone and urea or thiourea in the presence of N-(4-sulfonic acid) butyl triethyl ammonium hydrogen sulfate ([TEBSA][HSO4]) as the BrOnsted acidic ionic liquid and effective catalyst under thermal and solvent-free conditions. Good yields, short reaction times, straightforward workup, reusability of the catalyst, and green conditions are the most obvious advantages of this procedure.
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