4.3 Article

One-Pot Synthesis of 2-Amino-5,10-dihydro-5,10-dioxo-4-phenyl-4H-benzo[g]chromene Derivatives Catalyzed by ZnCl2

Journal

SYNTHETIC COMMUNICATIONS
Volume 41, Issue 6, Pages 806-811

Publisher

TAYLOR & FRANCIS INC
DOI: 10.1080/00397911003642666

Keywords

Benzo[g]chromene; cyanothioacetamide; lawsone; one-pot synthesis; ZnCl2

Funding

  1. University Grants Commission, New Delhi [32-201/2006 (SR)]

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[image omitted] An efficient one-pot synthesis of 2-amino-5,10-dihydro-5,10-dioxo-4-phenyl-4H-benzo[g]chromene derivatives has been achieved by the reaction of 2-hydroxynaphthalene-1,4-dione, cyanothioacetamide, and aromaticaldehyde in EtOH at room temperature catalyzed by ZnCl2. The structures of the products were characterized by infrared, 1H NMR, mass, and elemental analysis.

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