Journal
SYNTHETIC COMMUNICATIONS
Volume 39, Issue 13, Pages 2279-2287Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910802654716
Keywords
Hydrazide; hypervalent iodine; 1; 3; 4-oxadiazine; -tosyloxylation
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Funding
- Department of Science and Technology [SR/FTP/CS-77/2005]
- University Grants Commission, New Delhi, India [MRP 32-245/2006 SR]
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A novel and direct method for the efficient synthesis of 2,5-disubstituted 1,3,4-oxadiazines from the reactions of [hydroxy(tosyloxy)iodo]benzene with substituted acetophenones, followed by the treatment with acid hydrazide and K2CO3, is reported. The methodology is also extended to the synthesis of 5-aryl-6H-1,3,4-thiadiazin-2-amine by using thiosemicarbazide under similar experimental conditions.
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