Journal
SYNTHETIC COMMUNICATIONS
Volume 39, Issue 6, Pages 1065-1075Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910802474990
Keywords
Alkene functionalization; hypervalent iodine reagents; nitrene precursor; x-ray
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Funding
- European Union (EU) [FP6-NMP3-C-2003-505267]
- COST (European Cooperation in the field of Scientific and Technical Research) program
- GlaxoSmithKline
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Conditions for improved preparation of the crystalline iodine(III) reagents [1,2-C6H4(C(CF3)2OI)]2O and 1,2-C6H4(CH2OMe)(I=NTs) are presented together with their x-ray structures. The former is prepared by hydrolysis of 1,2-C6H4(C(CF3)2OICl (x-ray) and allows the preparation of cyclic sulfates from alkenes; the latter fashions sulfamidate under related conditions.
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