Journal
SYNTHETIC COMMUNICATIONS
Volume 38, Issue 17, Pages 2983-2994Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910802006396
Keywords
aluminum tris(dihydrogen phosphate); amidoalkyl naphthol; heterogeneous catalyst; multicomponent reaction; solvent-free
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Funding
- Sistan and Baluchestan University Research Council
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A new, facile, and cost-effective process involving the solvent-free synthesis of amidoalkyl naphthols using a three-component, one-pot condensation reaction of -naphthol, aromatic aldehyde, and amides in the presence of Al(H2PO4)(3) as heterogeneous catalyst under thermal conditions and microwave irradiation has been described. This new approach has the advantage of consistently excellent yields and short reaction times. The catalyst has shown a very stable catalytic activity in the reaction conditions and also can be recovered and recycled.
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