Journal
SYNTHESIS-STUTTGART
Volume 45, Issue 16, Pages 2323-2327Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0033-1339186
Keywords
thiophosphates; copper iodide; thiols; H-phosphonates; coupling
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Funding
- Institute for Advanced Studies in Basic Sciences (IASBS) Research Council [G2010IASBS120]
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A simple, efficient, and new method has been developed for the preparation of thiophosphates from benzenethiols. The method involves copper(I) iodide catalyzed coupling of thiols with H-phosphonates in the presence of triethylamine. The reaction proceeds effectively to afford the corresponding thiophosphates in moderate to good yields via an aerobic dehydrogenative coupling of H-phosphonates with benzenethiols. This method is easy, rapid, and good-yielding for the synthesis of thiophosphates from benzenethiols.
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