Journal
SYNTHESIS-STUTTGART
Volume -, Issue 9, Pages 1442-1446Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1259975
Keywords
5 '-deoxytubercidin; Vorbruggen glycosylation; pyrrolo[2,3-d]pyrimidine; marine nucleoside; 7-deazapurine
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Funding
- Chinese Ministry of Education
- NSF of China [20972086, 20962009]
- SRFDP [20090002110060]
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An efficient and practical synthesis of naturally occurring marine nucleosides 5'-deoxytubercidins on a 10 gram scale in good overall yield is reported. The key step was the Vorbruggen glycosylation of pyrrolo[2,3-d]pyrimidines with 5-deoxy-1,2,3-tri-O-acetyl-beta-D-ribofuranose.
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