Journal
SYNTHESIS-STUTTGART
Volume -, Issue 10, Pages 1541-1546Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1259998
Keywords
alkynes; catalysis; cross-coupling; alkadiynes
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Funding
- National Natural Science Foundation of China [20972057, 21002039]
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A simple synthesis of unsymmetrical buta-1,3-diynes by cross-coupling of terminal alkynes with 1-bromoalkynes in the presence of copper(I) iodide and tris(o-tolyl) phosphine was developed that gives good yields under simple and mild reaction conditions. The scope and limitations of the cross-coupling reaction were investigated.
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