Journal
SYNTHESIS-STUTTGART
Volume -, Issue 8, Pages 1283-1287Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2008-1072517
Keywords
thiocyanation; ketones; iron(III) chloride; catalysis; alpha-oxo thiocyanates
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A simple and efficient method for the alpha-thiocyanation of ketones has been developed; anhydrous iron(III) chloride is used under mild conditions to produce alpha-oxo thiocyanates in good to high yields and with high selectivity. The use of inexpensive and readily available iron(III) chloride makes this procedure simple, convenient, and practical.
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