Journal
SYNTHESIS-STUTTGART
Volume -, Issue 13, Pages 2023-2032Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2008-1067102
Keywords
Michael additions; reductions; thiols; triphenylphosphine; benzothiazepinones
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A tandem disulfide reduction-Michael addition was developed using both free and polymer-bound triphenylphosphine as the reducing agent. The procedure was applied to intermolecular systems for the synthesis of arylsulfanyl- and alkylsulfanyl- sub sti tuted propanoates and related ketones, and to an intramolecular system for the synthesis of a benzothiazepinone derivative.
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