Journal
SYNLETT
Volume 25, Issue 2, Pages 193-196Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0033-1340088
Keywords
pyridine; multicomponent reactions; zirconium; Krohnke pyridine; solvent-free
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Funding
- Research Affairs Office of Bu-Ali Sina University [32-1716]
- Center of Excellence in Development of Chemical Methods (CEDCM), Hamedan, I. R. Iran
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An efficient procedure for the synthesis of 2,4,6-triarylpyridines (Krohnke pyridines) by the one-pot multicomponent condensation of aldehydes (1 equiv) with acetophenones (2 equiv) and ammonium acetate (1.2 equiv) in the presence of catalytic amounts of oxozirconium(IV) chloride (ZrOCl2) under solvent-free conditions is described. In this work, four products have been reported for the first time. Easy work-up, simple methodology, clean reaction and reusability of the catalyst are some advantages of this work.
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