Journal
SYNLETT
Volume 24, Issue 8, Pages 955-958Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0032-1316899
Keywords
palhinine A; domino Michael reaction; X-ray crystal structure; Arndt-Eistert homologation; intramolecular aldol reaction
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Funding
- Deutsche Forschungsgemeinschaft
- Fonds der Chemischen Industrie
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A synthesis of the tricyclic partly substituted core structure of palhinine A was achieved. To reach the bicyclo[2.2.2]octane motif a domino Michael reaction was employed as a key step. After Arndt-Eistert homologation and intramolecular aldol reaction the isotwistane core could be obtained after simple functional-group manipulations.
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