Journal
SYNLETT
Volume -, Issue 11, Pages 1696-1700Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0031-1290406
Keywords
Mitsunobu reaction; esterification; hydrophobic tag; solid-phase extraction; inversion of configuration
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Funding
- National Natural Science Foundation of China [21072014]
- Ministry of Science and Technology of China [2012CB822100]
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A separation-friendly Mitsunobu reaction using hydrophobic-tagged acids is reported. Commercially available or simply prepared and recyclable hydrophobic-tagged acids can react with various alcohols to afford the target products in high yield with easy purification based on C-18 silica solid-phase extraction or normal silica gel filtration.
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