Journal
SYNLETT
Volume -, Issue 11, Pages 1585-1591Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1260795
Keywords
antimony(III) chloride; alkylation; arenes; microwave; oxygen heterocycles
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Funding
- GEQD, Hyderabad, DFS, MHA, Government of India
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An efficient protocol for alkylation of electron-rich arenes/heteroarenes with benzylic alcohols under microwave irradiation using antimony(III) chloride as catalyst has been developed. The mild reaction conditions, high yields, operational simplicity, and applicability to various substrates render the approach a useful route for the synthesis of diaryl/triarylalkane. In addition, a new route for the conversion of ortho-alkenylated phenols into functionalized O-heterocycles has been accomplished.
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