Journal
SYNLETT
Volume -, Issue 2, Pages 227-230Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1259295
Keywords
palladium; heterocycles; alkenols; alkoxylation; molecular oxygen
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Funding
- Ministero dell'Universita e della Ricerca [PRIN 2008KRBX3B]
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Synthesis of 1,4-2H-oxazine derivatives was performed by Pd(II)-catalyzed aerobic oxidative cyclization of 3-aza-5-alkenols, prepared from easily available 1,2-amino alcohols. The reaction proceeds in very mild conditions with a simple catalytic system consisting of PdCl2(MeCN)(2) in THF at room temperature with molecular oxygen as the sole stoichiometric oxidant.
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