Journal
SYNLETT
Volume -, Issue 19, Pages 2815-2818Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0031-1289566
Keywords
cyclization; heterocycles; heterogeneous catalysis; azides; alkynes
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Funding
- MEXT (Ministry of Education, Culture, Sports, Science, and Technology of the Japanese Government)
- Grants-in-Aid for Scientific Research [23790034] Funding Source: KAKEN
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A mixture of phenylmercuric acetate and trifluoromethanesulfonic acid or silica gel supported phenylmercuric trifluoromethanesulfonate (silaphenyl mercuric triflate) efficiently catalyzed the formation of pyrroles from homopropargyl azide derivatives. The reactions proceed using 20 mol% of the heterogeneous catalyst with yields of isolated pyrroles ranging from 74% to 99%.
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