Journal
SYNLETT
Volume -, Issue 15, Pages 2245-2247Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1261203
Keywords
inverse electron demand Diels-Alder; domino reaction; dibenzopyranone; urolithin M7
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Funding
- National Science and Engineering Research Council (NSERC) of Canada
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Urolithin M7 was synthesized from 2-hydroxy-4-methoxybenzaldehyde in 8 steps and 48% overall yield. The key step was an inverse electron demand Diels-Alder (IEDDA) reaction between diene 10 and the enamine (7) derived from dimethoxyacetaldehyde and pyrrolidine, which generated the 6H-dibenzo[b,d] pyran-6-one skeleton.
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