Journal
SYNLETT
Volume -, Issue 10, Pages 1467-1471Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1260759
Keywords
1,2,4-triazoles; hydrazonoyl hydrochloride; nitrilimine; 1,3-dipolar cycloaddition; oximes
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Funding
- China Medical University [CMU100-S-]
- National Science Council of Republic of China [NSC-99-2320-B-039-014-MY3]
- Taiwan Department of Health Clinical Trial and Research Center of Excellence [DOH100-TD-B-111-004]
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An effective 1,3-dipolar cycloaddition for the synthesis of 1,3,5-trisubstituted 1,2,4-triazole derivatives was developed by reacting oximes with hydrazonoyl hydrochlorides using triethylamine as a base. The desired 1,3,5-trisubstituted 1,2,4-triazoles were obtained in good yields and the reaction was applicable to aliphatic, cyclic aliphatic, aromatic and heterocyclic oxime substrates.
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