Journal
SYNLETT
Volume -, Issue 6, Pages 866-868Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0029-1219554
Keywords
piperidines; allenes; cyclisation; silver; alkaloids
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Funding
- Nanyang Technological University
- Singapore Ministry of Education Academic Research Fund Tier 2 [T206B1220RS]
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A highly diastereoselective silver-catalysed cyclisation of a 2-substituted beta-allenic hydroxylamine is reported. The resulting trans-isoxazolidine is converted into two Nuphar alkaloids by a sequence involving cross-metathesis and intramolecular reductive amination.
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