Journal
SYNLETT
Volume -, Issue 19, Pages 3099-3102Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0029-1218301
Keywords
marine sponge; glycolipid; mannose; glycosylation; inositol
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Funding
- EPSRC/University
- Royal Society
- AstraZeneca
- BBSRC
- St Hugh's College, Oxford
- EPSRC National Mass Spectrometry Service Centre, Swansea
- University of St Andrews NMR and Mass Spectrometry Services
- Biotechnology and Biological Sciences Research Council [BB/C515255/1] Funding Source: researchfish
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The first synthesis of the inositol-containing marine glycolipid dioctadecanoyl discoside is reported. The key glycosylation reaction proceeds with beta-selectivity at reduced temperature. The separable anomers could be readily progressed to afford discoside, its peracetate and the unnatural beta-derivatives.
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