Journal
SYNLETT
Volume -, Issue 4, Pages 623-627Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0029-1219160
Keywords
carbon disulfide; epoxide; aluminium; salen; dithiocarbonate; trithiocarbonate
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Funding
- Newcastle University
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The combination of a bimetallic aluminium(salen) complex and tetrabutylammonium bromide was found to catalyse the synthesis of cyclic di- and trithiocarbonates from epoxides and carbon disulfide. Reactions carried out at 50 degrees C produced 1,3-oxathiolane-2-thiones, whilst at 90 degrees C, 1,3-dithiolane-2-thiones were formed.
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