Journal
SYNLETT
Volume -, Issue 13, Pages 2188-2190Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0029-1217558
Keywords
Michael addition; nitroalkane; stemoamide; synthesis; unsaturated butyrolactone
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Funding
- NSFC [90713007, 20772141, 20625204, 20632030]
- MOST_863 [2006AA09Z405, 2006AA09Z446]
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We describe a practical synthesis of (+)-9a-epi-stemoamide, which has been achieved in six steps from a,p-unsaturated gamma-butyrolactone. The main features of the current approach include a DBU-catalyzed Michael addition of nitroalkane and a reductive lactamization of nitro esters.
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