Journal
FARADAY DISCUSSIONS
Volume 180, Issue -, Pages 35-53Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5fd00003c
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Funding
- Lawrence Berkeley National Laboratory
- Office of Science, Office of Basic Energy Sciences of the US Department of Energy at the Lawrence Berkeley National Laboratory [DE-AC02-05CH11231]
- Office of Science, Office of Basic Energy Sciences
- Division of Chemical Sciences, Geosciences, and Biosciences of the US Department of Energy at the Lawrence Berkeley National Laboratory [DE-AC02-05CH11231]
- DOE Division of Materials Sciences [DE-AC02-05CH11231]
- ARO-MURI [W911-NF-09-1-0398]
- Deutscher Akademischer Austauschdienst (DAAD)
- Wenner-Gren Foundations in Stockholm, Sweden
- French LabEx PALM, APTCOM Project [ANR-10-LABX-0039]
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We describe a new in operando approach for the investigation of heterogeneous processes at solid/liquid interfaces with elemental and chemical specificity which combines the preparation of thin liquid films using the meniscus method with standing wave ambient pressure X-ray photoelectron spectroscopy [Nemsak et al., Nat. Commun., 5, 5441 (2014)]. This technique provides information about the chemical composition across liquid/solid interfaces with sub-nanometer depth resolution and under realistic conditions of solution composition and concentration, pH, as well as electrical bias. In this article, we discuss the basics of the technique and present the first results of measurements on KOH/Ni interfaces.
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