Journal
SUPRAMOLECULAR CHEMISTRY
Volume 24, Issue 4, Pages 279-284Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/10610278.2012.658393
Keywords
bridged calix[6]arenes; bisdioxine spacer; conformation; X-ray structure
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Funding
- Karl Franzens Universitat Graz
- University of Queensland
- Australian Research Council
- UQ
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The novel 1,2-bridged calix[6]arene 5 is prepared in a cyclocondensation reaction of 1,3,5,7-tetra-tert-butyl-2,6,9-trioxabicyclo[3.3.1]nona-3,7-diene-4,8-dicarbonylchloride ('bisdioxine') 2 with p-tert-butylcalix[6] arene. Elucidation of its structure is based on an X-ray structure determination together with supporting NMR and MS investigations. The new macrocycle 5 offers good complexation properties for Cs+ ions.
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