Journal
SUPERCONDUCTOR SCIENCE & TECHNOLOGY
Volume 22, Issue 1, Pages -Publisher
IOP PUBLISHING LTD
DOI: 10.1088/0953-2048/22/1/015020
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Funding
- National Key Basic Research [2006CB601005, 2007CB925002]
- National Nature Science Foundation of China [10774146, 10774147]
- Director's Fund of Hefei Institutes of Physical Science
- Chinese Academy of Sciences
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In this work, crystals of FeSex have been grown by a flux approach. The crystallization process is divided into two stages. First, stoichiometric polycrystal FeSe0.82 was sintered in a solid state reaction. Then, FeSex crystals with a size about 500 mu m were successfully grown in an evacuated sealed quartz tube using a NaCl/KCl flux. The products include two crystal structures: tetragonal and hexagonal. The electronic transport and magnetic property measurements show that FeSex crystals exhibit a superconducting transition at about 10 K.
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