Journal
SCIENCEASIA
Volume 38, Issue 3, Pages 295-300Publisher
SCIENCE SOCIETY THAILAND
DOI: 10.2306/scienceasia1513-1874.2012.38.295
Keywords
amorphous silica; metakaolin; alkaline fusion method; incubation
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Funding
- Thailand Research Fund by the Science Achievement Scholarship of Thailand (SAST)
- Faculty of Science and the Graduate School of Chiang Mai University
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In this study, a Na-x zeolite was synthesized by using metakaolin from Narathiwat kaolinite, amorphous silica from rice husk ash, and high CaO fly ash from the Mae Moh electrical plant by using the alkaline fusion method. The mixture of fly ash, amorphous silica and metakaolin was fused in NaOH followed by incubation at 70 degrees C for 24 h. An amorphous silica from rice husk ash and metakaolin were added to high CaO fly ash to increase the SiO2/Al2O3 ratio of fusion materials. The fused mixtures of high CaO fly ash, amorphous silica and metakaolin were mixed in the weight ratio of 1:3:6 giving a SiO2/Al2O3 ratio of 3.25 to achieve a Na-x zeolite phase. The synthesized zeolite was characterized by XRD, SEM, FTIR, and BET techniques. The CEC and specific surface area of the Na-x zeolite were 420 meq 100 g(-1) and 398 m(2)/g, respectively.
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