Journal
RSC ADVANCES
Volume 5, Issue 33, Pages 25642-25649Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra02972d
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- University of Kuwait [SC03/14]
- facility of ANALAB
- facility of SAF [GS01/01, GS01/05, GS01/03, GS03/08]
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The 1,3-dipolar cycloaddition reaction of the bis-hydrazonoyl chlorides with 2-arylidene-1-benzosuberone derivatives afforded the corresponding bis-[1',4'-diaryl-1-oxo-spiro-benzosuberane-2,5'-pyrazoline] derivatives. The reaction is carried out under ultrasonic irradiation as well as under conventional heating. The factors affecting the optimization of the cycloaddition reaction are examined in detail. X-ray crystallographic analysis was used in the establishment of the regio- and stereochemistry of the cycloaddition products.
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