Journal
RSC ADVANCES
Volume 5, Issue 23, Pages 18035-18040Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ra16284f
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Funding
- Spanish MINECO [MAT2010-15870]
- Aragon Government
- ESF
- FPU Program fellowships
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A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm(2) section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent.
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