Journal
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
Volume 58, Issue 4, Pages 411-415Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023613040190
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Neutral [EuL(3)Phen] complexes were synthesized by the reaction of EuCl3 with heterocyclic diketones-1-(1,5-dimethyl-1H-pyrazol-4-yl)-4,4,4-trifluoro-1,3-butanedione and 4,4,5,5,6,6,6-heptafluoro-1-(1-methyl-1H-pyrazol-4-yl)-1,3-hexanedione-and 1,10-phenanthroline (Phen) in an aqueous alcohol solution in the presence of NaOH. The reaction of GdCl3 with the same diketones under analogous conditions, but without adding 1,10-phenanthroline, yielded [GdL3(H2O)(2)] complexes. The composition of the complexes was determined by elemental analysis, and their optical and luminescent properties were examined.
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