Journal
RUSSIAN CHEMICAL BULLETIN
Volume 57, Issue 12, Pages 2535-2539Publisher
SPRINGER
DOI: 10.1007/s11172-008-0364-5
Keywords
carboranes; enantiomers; HPLC; chiral stationary phases; kinetic resolution
Categories
Funding
- Russian Foundation for Basic Research [07-03-00684]
- International Scientific and Technical Center [3477]
- Russian Federation President Council [NSh 3758.2008.3]
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A determination of enantiomeric purity of 1-substituted (Me, Ph, and Pr-i) 3-amino-1,2dicarba-closo-dodecaboranes by HPLC on chiral Chiralcel OD-H and Chiralpac AD stationary phases involving preliminary phthaloylation of 3-aminocarboranes has been suggested as a general method.
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