4.5 Article

A multi-crystal wavelength dispersive x-ray spectrometer

Journal

REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 83, Issue 7, Pages -

Publisher

AMER INST PHYSICS
DOI: 10.1063/1.4737630

Keywords

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Funding

  1. National Institutes of Health (NIH) [GM 55302]
  2. National Institute of General Medical Sciences (NEGMS) [P41GM103393]
  3. National Center for Research Resources (NCRR) [P41RR001209]
  4. National Science Foundation (NSF) [CHE-0809324]
  5. Alexander von Humboldt Foundation
  6. AMOS within the Chemical Sciences division of the Office of Basic Energy Sciences, Office of Science, U.S. Department of Energy (DOE)
  7. Office of Science, Office of Basic Energy Sciences, Division of Chemical Sciences, Geosciences, and Biosciences (CSGB) of the DOE [DE-AC02-05CH11231]

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A multi-crystal wavelength dispersive hard x-ray spectrometer with high-energy resolution and large solid angle collection is described. The instrument is specifically designed for time-resolved applications of x-ray emission spectroscopy (XES) and x-ray Raman scattering (XRS) at X-ray Free Electron Lasers (XFEL) and synchrotron radiation facilities. It also simplifies resonant inelastic x-ray scattering (RIXS) studies of the whole 2d RIXS plane. The spectrometer is based on the Von Hamos geometry. This dispersive setup enables an XES or XRS spectrum to be measured in a single-shot mode, overcoming the scanning needs of the Rowland circle spectrometers. In conjunction with the XFEL temporal profile and high-flux, it is a powerful tool for studying the dynamics of time-dependent systems. Photo-induced processes and fast catalytic reaction kinetics, ranging from femtoseconds to milliseconds, will be resolvable in a wide array of systems circumventing radiation damage. (C) 2012 American Institute of Physics. [http://dx.doi.org/10.1063/1.4737630]

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