Journal
REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 81, Issue 7, Pages -Publisher
AMER INST PHYSICS
DOI: 10.1063/1.3455178
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- Access to Major Research Facilities Programme [08/09-N-22]
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We describe the design and use of a closed three-electrode electrochemical cell for neutron reflectometry studies of the structure of the electrical double-layer in ionic liquids. A transparent glass counter electrode was incorporated to allow easy monitoring of any gas bubbles trapped in the cell. A 100 mm diameter silicon wafer polished to 0.1 nm rms roughness coated with gold over a chromium adhesion layer was used as the working electrode. The utility of the cell was demonstrated during neutron reflectometry measurements of the ultrahigh purity ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide ([C(4)mpyr][NTf2]) at two different applied potentials. (C) 2010 American Institute of Physics. [doi:10.1063/1.3455178]
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