Journal
RESEARCH ON CHEMICAL INTERMEDIATES
Volume 41, Issue 7, Pages 4283-4292Publisher
SPRINGER
DOI: 10.1007/s11164-013-1529-x
Keywords
2-Aminothiophenol; Aldehydes; 2-Aryl/heteroaryl/styryl/alkylbenzothiazoles; Nitric acid; Silica gel
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Funding
- Haryana State Council of Science and Technology
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The present work was undertaken to develop an economic method for the synthesis of 2-aryl/heteroaryl/styryl/alkylbenzothiazoles mediated by SiO2-HNO3. In this report, we have demonstrated the catalytic potential of SiO2-HNO3 for the oxidative condensation of 2-aminothiophenol and aldehydes. Instant reaction at room temperature under solvent-free condition, high substrate to catalyst ratio 50:1 (by weight), practical application by large-scale synthesis, and excellent yields are the main advantages of the present protocol.
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