Journal
RESEARCH ON CHEMICAL INTERMEDIATES
Volume 38, Issue 3-5, Pages 1091-1099Publisher
SPRINGER
DOI: 10.1007/s11164-011-0445-1
Keywords
2,3-Dihydroquinazolin-4(1H)-ones; Aluminum methanesulfonate; Multicomponent reactions; Isatoic anhydride
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Funding
- Committee of Science and Technology of Liaoning Province of China [20091001]
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A wide range of mono- and disubstituted 2,3-dihydroquinazolin-4(1H)-ones were synthesized via a one-pot three components condensation of isatoic anhydride, aldehydes, and ammonium salts or primary amines in the presence of aluminum methanesulfonate in EtOH/H2O solution. The catalyst is reusable and could be recycled for several runs without any distinct decrease in its efficiency. A plausible mechanism for this one-pot three components reaction was proposed.
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