Journal
QUIMICA NOVA
Volume 36, Issue 4, Pages 577-U143Publisher
SOC BRASILEIRA QUIMICA
DOI: 10.1590/S0100-40422013000400016
Keywords
ultrafast 2D NMR; COSY; HSQC
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Funding
- Agence Nationale de la Recherche (ANR) [2010-JCJC-0804-01]
- Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES)
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq)
- Fundacao de Amparo a Pesquisa do Estado de Sao Paulo (FAPESP)
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Ultrafast 2D NMR is a powerful methodology that allows recording of a 2D NMR spectrum in a fraction of second. However, due to the numerous non-conventional parameters involved in this methodology its implementation is no trivial task. Here, an optimized experimental protocol is carefully described to ensure efficient implementation of ultrafast NMR. The ultrafast spectra resulting from this implementation are presented based on the example of two widely used 2D NMR experiments, COSY and HSQC, obtained in 0.2 s and 41 s, respectively.
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