Journal
PROPELLANTS EXPLOSIVES PYROTECHNICS
Volume 35, Issue 4, Pages 395-406Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/prep.200900058
Keywords
Energetic Materials; Nitrogen-Rich Salts; Tetrazoles; X-Ray Diffractometry
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Funding
- Ludwig-Maximilian University of Munich (LMU)
- Fonds der Chemischen Industrie (FCI)
- European Research Office (ERO) of the US Army Research Laboratory (ARL)
- Armament Research, Development and Engineering Center (ARDEC) [W911NF-09-2-0018, W911NF-09-1-0120, W011NF-09-1-0056]
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The compounds barium tetrazolate (6). ban urn 5-ammotettazolate tetrahydiate (7). barium 5-nitriminotetrazolate dihydrate (8), barium bis(1H-5-nitriminotetrazolate) tetrahydrate (9). barium 1-methy1-5-mtrimmotetrazolate monohydrate (10). and barium 2-methyl-5-nitriminotetrazolate dihydrate (11) were synthesized by the reactions of barium hydroxide octahydrate and 1H-tetrazole (1). 5-aminotetrazole (2). 1.4H-5-nitriminotetrazole (3). 1-methyl-5-nitriminotetrazole (4), and 2-methyl-5-nitriminotetrazole (5). respectively The compounds were characterized using multi-nuclear NMR spectroscopy. vibrational (IR and Raman) spectroscopy. elemental analysis. and differential scanning calorimetry The solid-state structures of 7-11 weft. (determined using low temperature X-ray diffraction and a comprehensive characterization is given In addition, the sensitivities (impact. fiction. electrical discharge) of 6-11 were investigated and bomb calorimetric measurements were carried out.
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