Journal
POLYMER CHEMISTRY
Volume 2, Issue 4, Pages 805-811Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0py00412j
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- CSIR, New Delhi
- CSIR [NWP0051-C]
- DST, New Delhi
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The novel synthesis of O-glycosylated lysine-NCA from a stable glycosyl donor and a commercially available protected amino acid in very high yield is reported. These O-glycosylated lysine-NCA monomers underwent ring opening polymerization using simple primary amine initiators to form well defined, high molecular weight homoglycopolypeptides and diblock co-glycopolypeptides. The synthesis of azide labelled end functionalized glycopolypeptides and amphiphilic diblock copolypeptides is also reported. This methodology represents an easy and practical route to the synthesis of O-glycosylated polypeptides with 100% glycosylation.
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