Journal
POLYMER
Volume 55, Issue 14, Pages 3083-3086Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.polymer.2014.05.036
Keywords
Ultrasound; Suzuki coupling reaction; Polyfluorene
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Funding
- National Basic Research Program of China (973 Program) [2013CB834701]
- National Science Foundation of China [21174050, 21374038]
- Ministry of Science and Technology of China [2009CB623605]
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Ultrasound-assisted synthesis of conjugated polymer is reported taking PF as an example. It is found that ultrasound can dramatically accelerate the Suzuki coupling reaction. The effects of ultrasonic amplitude, time, monomer and catalyst's concentration on the polymerization have been investigated. PF with high M-w, of 39,100 g/mol is obtained in 20 min under optimized condition. (C) 2014 Elsevier Ltd. All rights reserved.
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