Journal
POLYHEDRON
Volume 41, Issue 1, Pages 115-119Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.poly.2012.04.032
Keywords
Electrochemical synthesis; Zinc(II) complexes; Hexadentate amide-thioether; X-ray structure
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Funding
- Research Council of the University of Isfahan
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Three novel complexes of zinc with hexadentate amide-thioether ligands were synthesized by electrochemical oxidation of zinc in dichloromethane-methanol solution. These compounds were characterized by elemental analyses, H-1 NMR, and IR spectroscopy. The molecular structures of two complexes were determined by single crystal X-ray diffraction, indicating that, the metal atom is in a distorted octahedral environment with amide-thioether ligand acting as a hexadentate N2N'S-2(2) donor. (c) 2012 Elsevier Ltd. All rights reserved.
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