Journal
POLYHEDRON
Volume 27, Issue 11, Pages 2309-2314Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.poly.2008.04.033
Keywords
mercury; X-ray diffraction; N-inverted N-methylated porphyrin; (1)H relaxation
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The reaction of PhHgOAc with 2-NCH(3)NCTPPH (2) gave a mercury(II) complex of (phenylato)(2-N-methyl-5,10.15,20-tetraphenyl-21-carbaporphyrinato-N,N',N '')-mercury(II), [HgPh(2-NCH(3)NCTPP); 7]: the coordination sphere around Hg(1) in 7 was a four-coordinate derivative with a seesaw geometry and dipole-dipole (DD) interaction governed the longitudinal relaxation rate for Hg(1)-Ph-H(2,6) protons of 7 in CDCl(3) (0.01 M) at 599.95 MHz. (C) 2008 Elsevier Ltd. All rights reserved.
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