Journal
PHYSICAL REVIEW B
Volume 79, Issue 6, Pages -Publisher
AMER PHYSICAL SOC
DOI: 10.1103/PhysRevB.79.064504
Keywords
antiferromagnetic materials; barium compounds; crystal growth from solution; crystal structure; high-temperature superconductors; iron compounds; magnetic moments; magnetic structure; magnetic superconductors; Neel temperature; neutron diffraction; solid-state phase transformations; tin compounds; X-ray diffraction
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Antiferromagnetic ordering and structural phase transition have been investigated via comprehensive neutron and x-ray diffraction on Sn-flux-grown BaFe2As2 single crystals, the A-122 family of FeAs-based high-T-C superconductor compounds. The incorporation of Sn in the lattice resulted to an average composition of Ba0.95Sn0.05Fe2As2. A tetragonal-to-orthorhombic structural phase transition and a three-dimensional long-range antiferromagnetic ordering of the iron magnetic moment, with a unique magnetic propagation wave vector k=(1,0,1) have been found to take place at similar to 90 K. The magnetic moments of iron are aligned along the longer a axis in the low-temperature orthorhombic phase (Fmmm with b < a < c). Our results thus demonstrate that the magnetic structure of the Sn-flux-grown BaFe2As2 single crystal is the same as those in the polycrystalline samples and in other A-122 iron pnictides compounds. We argue that the Sn incorporation in the lattice is responsible for a smaller orthorhombic splitting and lower Neel temperature T-N observed in the experiments.
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